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Nar Sosunda Kromatografik Yöntemle Bazı Polisiklik Aromatik Hidrokarbonların Analizi

Yıl 2017, Cilt: 15 Sayı: 3, 269 - 273, 22.10.2017

Bugra Dayi Hatice Ardağ Akdoğan Abdullah Akdoğan

https://doi.org/10.24323/akademik-gida.345264
Cited By: 2

Öz

Polisiklik aromatik
hidrokarbonlar (PAH), insanlar ve hayvanlar için son derece toksik özellikte ve
kanserojendir. Bu bağlamda güvenli gıda üretimi açısından, üretimi yapılan
ticari nar soslarında bu bileşiklerin oluşumu ve düzeyleri önemli bir konudur.
Bu çalışmada Türkiye’de satışa sunulan sekiz farklı nar sosu kullanılmıştır. Yüksek
Performanslı Sıvı kromatografi-UV detektör (HPLC-UV) ile on üç tane PAH analizi
yapılmıştır. Sekiz farklı nar sosu örneği için basit, hassas ve maliyeti düşük
bir katı faz ekstraksiyonu (SPE) tekniği kullanılarak, PAH’ların ön deriştirilmesi
gerçekleştirilmiştir. Nar sosu numunelerinin optimum SPE koşullarında elde
edilen ekstraktları, daha sonra ters fazlı HPLC-UV dedektörü ile analiz
edilmiştir. Veriler değerlendirildiğinde, toplam PAH miktarları 1.5 mg/L ile 16.6
mg/L arasında değiştiği tespit edildi.

Anahtar Kelimeler

HPLC Polisiklik aromatik hidrokarbonlar Nar Nar sosları

Kaynakça

  • [1] Alessandra, M., Andrea, C., Eugenio, L., Luciana, M, Patrizia, P., Stefania, C., 2016. Evaluation of different extraction methods from pomegranate whole fruit or peels and the antioxidant and antiproliferative activity of the polyphenolic fraction. Food Chemistry 202: 59–69.
  • [2] Maskan, M., 2006. Production of pomegranate (Punica granatum L.) juice concentrate by various heating methods: colour degradation and kinetics. Journal of Food Engineering 72(3): 218-224.
  • [3] Vardin, H., Fenercioglu, H., 2003. Study on the development of pomegranate juice processing technology: clarification of pomegranate juice. National Center for Biotechnology Information 47(5): 300-3.
  • [4] Cemeroglu, B., Artik., N., Erbas, S., 1992 Gewinnung von Granatapfelsaft und seine Zusammensetzung. Flussiges Obst 59(6): 335-340.
  • [5] Hamid, R.R., Mohammad, A., Seyed, N.O., 2012. A comprehensive review of Punica granatum (pomegranate) properties in toxicological, pharmacological, cellular and molecular biology Researches. Iran Journal of Pharmaceutical Research 11(2): 385–400.
  • [6] Barranco, A., Alonso-Salces, R.M., Bakkali, A., Berrueta, L.A., Gallo, B., Vicente, F., Sarobe, M., 2003. Solid-phase clean-up in the liquid chromatographic determination of polycyclic aromatic hydrocarbons in edible oils. Journal of Chromatography A 988(1): 33-37.
  • [7] Busetti, F., Heitz, A., Cuomo, M., Badoer, S., Traverso, P., 2006. Determination of sixteen polycyclic aromatic hydrocarbons in aqueous and solid samples from an Italian wastewater treatment plant. Journal of Chromatography A 1102(1-2): 104-115.
  • [8] Simko, P., 2002. Determination of polycyclic aromatic hydrocarbons in smoked meat products and smoke favouring food additives. Journal of Chromatography B 770(1-2): 3-18.
  • [9] Tehranifar, A., Selahvarzi, Y., Kharrazi, M., Bakhsh, V.J., 2011. High potential of agroindustrial by-products of pomegranate (Punica granatum L.) as the powerful antifungal and antioxidant substances. Industrial Crops and Products 34(3): 1523-1527.
  • [10] Macek, T., Mackova, M., Kas, J., 2000. Exploitation of plants for the removal of organics in environmental remediation. Biotechnology Advances 18(1): 23-34.
  • [11] Mackova, M., Dowling, D.N., Macek. T., 2006. Phytoremediation and rhizoremediation. Focus on Biotechnology, vol. 9A. Springer, Dordrecht, The Netherlands.
  • [12] Harvey, P.J., Campanella, B.F., Castro, P.M.L., Harms, H., Lichtfouse, E., Schauffner, A.R., Smrcek, S., Werck-Reichhart, D., 2002. Phytoremediation of polyaromatic hydrocarbons, anilines and phenols. Environmental Science and Pollution Research 9(1): 29-47.
  • [13] Rezek, J., Wiesche, C., Mackova, M., Zadrazil, F., Macek, T., 2008. The effect of ryegrass (Lolium perenne) on decrease of PAH content in long term contaminated soil. Chemosphere 70(9): 1603-1608. [14] Shami, S.G., Wolff, R.K., Hahn, F.F., Brooks, A.L., Griffith, W.C., 1985. Early cytokinetic and morphological response of rat lungs to inhaled benzo(a)pyrene, gallium oxide, and SO2. Environmental Research 37(1): 12-25.
  • [15] Kira, S., Sakano, M., Nugami, Y., 1997. Measurement of a time-weighted average concentration of polycyclic aromatic hydrocarbons in aquatic environment using solid phase extraction cartridges and a portable pump. Bullettin of Environmental Contamination and Toxicology. 58(6): 878-884.
  • [16] Masih, A., Taneja, A., 2006. Polycyclic aromatic hydrocarbons (PAHs) concentrations and related carcinogenic potencies in soil at a semi-arid region of India. Chemosphere 65(3): 449-456.
  • [17] Countway, R.E., Dickhut, RM., Canuel, E.A., 2003. Polycyclic aromatic hydrocarbon (PAH) distribution and associations with organic matter in surface waters of the York River, VA Estuary. Organic Geochemistry 34(2): 209-224.
  • [18] Luthe, G., Broeders, J., Brinkman, U.A.T.H., 2001. Mono fluorinated polycyclic aromatic hydrocarbons as internal standards to monitor trace enrichment and desrption of their parent compound during solid-phase extraction. Journal of Chromatography A 933(1-2): 27-35.
  • [19] World Health Organization Regional Office for Europe, 1987. Polynuclear aromatic hydrocarbons (PAH), Air quality guidelines for Europe; Copenhagen, 105-117.

Chromatographic Analysis of Polycyclic Aromatic Hydrocarbons in Pomegranate Sauces

Yıl 2017, Cilt: 15 Sayı: 3, 269 - 273, 22.10.2017

Bugra Dayi Hatice Ardağ Akdoğan Abdullah Akdoğan

https://doi.org/10.24323/akademik-gida.345264
Cited By: 2

Öz

Polycyclic aromatic
hydrocarbons (PAH) are highly toxic and carcinogenic to humans and animals. In
terms of safe food production, the formation and levels of these compounds in
commercial pomegranate sauces are important. This study was carried out on
eight different pomegranate sauces sold in Turkey. Thirteen PAH analyzes were
performed with High Performance Liquid Chromatography-UV detector (HPLC-UV).
Pre-concentration of PAHs was performed by a simple, precise and low cost solid
phase extraction (SPE) technique for eight different pomegranate sauces
samples. Extracts of pomegranate sauce samples obtained under optimum SPE
conditions were then analyzed by reversed-phase HPLC-UV detector. Results
indicated that the total amounts of PAHs varied from 1.5 mg/L to 16.6 mg/L.

Anahtar Kelimeler

HPLC Polycyclic aromatic hydrocarbons Pomegranate Pomegranate sauces

Kaynakça

  • [1] Alessandra, M., Andrea, C., Eugenio, L., Luciana, M, Patrizia, P., Stefania, C., 2016. Evaluation of different extraction methods from pomegranate whole fruit or peels and the antioxidant and antiproliferative activity of the polyphenolic fraction. Food Chemistry 202: 59–69.
  • [2] Maskan, M., 2006. Production of pomegranate (Punica granatum L.) juice concentrate by various heating methods: colour degradation and kinetics. Journal of Food Engineering 72(3): 218-224.
  • [3] Vardin, H., Fenercioglu, H., 2003. Study on the development of pomegranate juice processing technology: clarification of pomegranate juice. National Center for Biotechnology Information 47(5): 300-3.
  • [4] Cemeroglu, B., Artik., N., Erbas, S., 1992 Gewinnung von Granatapfelsaft und seine Zusammensetzung. Flussiges Obst 59(6): 335-340.
  • [5] Hamid, R.R., Mohammad, A., Seyed, N.O., 2012. A comprehensive review of Punica granatum (pomegranate) properties in toxicological, pharmacological, cellular and molecular biology Researches. Iran Journal of Pharmaceutical Research 11(2): 385–400.
  • [6] Barranco, A., Alonso-Salces, R.M., Bakkali, A., Berrueta, L.A., Gallo, B., Vicente, F., Sarobe, M., 2003. Solid-phase clean-up in the liquid chromatographic determination of polycyclic aromatic hydrocarbons in edible oils. Journal of Chromatography A 988(1): 33-37.
  • [7] Busetti, F., Heitz, A., Cuomo, M., Badoer, S., Traverso, P., 2006. Determination of sixteen polycyclic aromatic hydrocarbons in aqueous and solid samples from an Italian wastewater treatment plant. Journal of Chromatography A 1102(1-2): 104-115.
  • [8] Simko, P., 2002. Determination of polycyclic aromatic hydrocarbons in smoked meat products and smoke favouring food additives. Journal of Chromatography B 770(1-2): 3-18.
  • [9] Tehranifar, A., Selahvarzi, Y., Kharrazi, M., Bakhsh, V.J., 2011. High potential of agroindustrial by-products of pomegranate (Punica granatum L.) as the powerful antifungal and antioxidant substances. Industrial Crops and Products 34(3): 1523-1527.
  • [10] Macek, T., Mackova, M., Kas, J., 2000. Exploitation of plants for the removal of organics in environmental remediation. Biotechnology Advances 18(1): 23-34.
  • [11] Mackova, M., Dowling, D.N., Macek. T., 2006. Phytoremediation and rhizoremediation. Focus on Biotechnology, vol. 9A. Springer, Dordrecht, The Netherlands.
  • [12] Harvey, P.J., Campanella, B.F., Castro, P.M.L., Harms, H., Lichtfouse, E., Schauffner, A.R., Smrcek, S., Werck-Reichhart, D., 2002. Phytoremediation of polyaromatic hydrocarbons, anilines and phenols. Environmental Science and Pollution Research 9(1): 29-47.
  • [13] Rezek, J., Wiesche, C., Mackova, M., Zadrazil, F., Macek, T., 2008. The effect of ryegrass (Lolium perenne) on decrease of PAH content in long term contaminated soil. Chemosphere 70(9): 1603-1608. [14] Shami, S.G., Wolff, R.K., Hahn, F.F., Brooks, A.L., Griffith, W.C., 1985. Early cytokinetic and morphological response of rat lungs to inhaled benzo(a)pyrene, gallium oxide, and SO2. Environmental Research 37(1): 12-25.
  • [15] Kira, S., Sakano, M., Nugami, Y., 1997. Measurement of a time-weighted average concentration of polycyclic aromatic hydrocarbons in aquatic environment using solid phase extraction cartridges and a portable pump. Bullettin of Environmental Contamination and Toxicology. 58(6): 878-884.
  • [16] Masih, A., Taneja, A., 2006. Polycyclic aromatic hydrocarbons (PAHs) concentrations and related carcinogenic potencies in soil at a semi-arid region of India. Chemosphere 65(3): 449-456.
  • [17] Countway, R.E., Dickhut, RM., Canuel, E.A., 2003. Polycyclic aromatic hydrocarbon (PAH) distribution and associations with organic matter in surface waters of the York River, VA Estuary. Organic Geochemistry 34(2): 209-224.
  • [18] Luthe, G., Broeders, J., Brinkman, U.A.T.H., 2001. Mono fluorinated polycyclic aromatic hydrocarbons as internal standards to monitor trace enrichment and desrption of their parent compound during solid-phase extraction. Journal of Chromatography A 933(1-2): 27-35.
  • [19] World Health Organization Regional Office for Europe, 1987. Polynuclear aromatic hydrocarbons (PAH), Air quality guidelines for Europe; Copenhagen, 105-117.
Toplam 18 adet kaynakça vardır.

Ayrıntılar

Bölüm Araştırma Makaleleri
Yazarlar

Bugra Dayi Bu kişi benim

Hatice Ardağ Akdoğan

Abdullah Akdoğan

Yayımlanma Tarihi 22 Ekim 2017
Gönderilme Tarihi 20 Ekim 2017
Yayımlandığı Sayı Yıl 2017 Cilt: 15 Sayı: 3

Kaynak Göster

APA Dayi, B., Ardağ Akdoğan, H., & Akdoğan, A. (2017). Nar Sosunda Kromatografik Yöntemle Bazı Polisiklik Aromatik Hidrokarbonların Analizi. Akademik Gıda, 15(3), 269-273. https://doi.org/10.24323/akademik-gida.345264
AMA Dayi B, Ardağ Akdoğan H, Akdoğan A. Nar Sosunda Kromatografik Yöntemle Bazı Polisiklik Aromatik Hidrokarbonların Analizi. Akademik Gıda. Ekim 2017;15(3):269-273. doi:10.24323/akademik-gida.345264
Chicago Dayi, Bugra, Hatice Ardağ Akdoğan, ve Abdullah Akdoğan. “Nar Sosunda Kromatografik Yöntemle Bazı Polisiklik Aromatik Hidrokarbonların Analizi”. Akademik Gıda 15, sy. 3 (Ekim 2017): 269-73. https://doi.org/10.24323/akademik-gida.345264.
EndNote Dayi B, Ardağ Akdoğan H, Akdoğan A (01 Ekim 2017) Nar Sosunda Kromatografik Yöntemle Bazı Polisiklik Aromatik Hidrokarbonların Analizi. Akademik Gıda 15 3 269–273.
IEEE B. Dayi, H. Ardağ Akdoğan, ve A. Akdoğan, “Nar Sosunda Kromatografik Yöntemle Bazı Polisiklik Aromatik Hidrokarbonların Analizi”, Akademik Gıda, c. 15, sy. 3, ss. 269–273, 2017, doi: 10.24323/akademik-gida.345264.
ISNAD Dayi, Bugra vd. “Nar Sosunda Kromatografik Yöntemle Bazı Polisiklik Aromatik Hidrokarbonların Analizi”. Akademik Gıda 15/3 (Ekim 2017), 269-273. https://doi.org/10.24323/akademik-gida.345264.
JAMA Dayi B, Ardağ Akdoğan H, Akdoğan A. Nar Sosunda Kromatografik Yöntemle Bazı Polisiklik Aromatik Hidrokarbonların Analizi. Akademik Gıda. 2017;15:269–273.
MLA Dayi, Bugra vd. “Nar Sosunda Kromatografik Yöntemle Bazı Polisiklik Aromatik Hidrokarbonların Analizi”. Akademik Gıda, c. 15, sy. 3, 2017, ss. 269-73, doi:10.24323/akademik-gida.345264.
Vancouver Dayi B, Ardağ Akdoğan H, Akdoğan A. Nar Sosunda Kromatografik Yöntemle Bazı Polisiklik Aromatik Hidrokarbonların Analizi. Akademik Gıda. 2017;15(3):269-73.

Cited By

Determination of Physical, Chemical and Antioxidant Properties of Pomegranate Sauces Sold in The Market in Turkey
Turkish Journal of Analytical Chemistry
https://doi.org/10.51435/turkjac.1127473
Bazı Et Türlerinde Polisiklik Aromatik Hidrokarbon Oluşumuna Farklı Pişirme Yöntemlerinin Etkisi
Akademik Gıda
Ömer Şerif Aydın
https://doi.org/10.24323/akademik-gida.505505

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