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Year 2019, Volume: 3 Issue: 3, 195 - 201, 15.12.2019

Hakan Gökmeşe Bulent Bostan Talha Alper Yilmaz Ufuk Tasci

https://doi.org/10.35860/iarej.630999
Cited By: 4

Abstract

References

  • 1. Sivasankaran, S., Sivaprasad, K., Narayanasamy, R., Satyanarayana, P.V., X-ray peak broadening analysis of AA 6061100 −x−x wt.% Al2O3 nanocomposite prepared by mechanical alloying, Materials Characterization, 2011. 62: 661-672.
  • 2. Khaghani-Dehaghani M.A., Ebrahimi-Kahrizsangi R., Setoudeh N., Nasiri-Tabrizi B., Mechanochemical synthesis of Al2O3–TiB2 nanocomposite powder from Al–TiO2–H3BO3 mixture, Int. Journal of Refractory Metals and Hard Materials, , 2011. 29: 244–249.
  • 3. Yokoyama, T., Basic Properties and Measuring Methods of Nanoparticles, Fundamentals of Nanoparticles, 2013. Chapter 1, 5-10.
  • 4. Castro, C. L. and Mitchell, B. S. Nanoparticles from Mechanical Attrition, Functionalization and Surface Treatment of Nanoparticles, 2002. Chapter 1, 1-15.
  • 5. Rahimian, M., Ehsania, N., Parvin, N., Baharvandi, H. R., The effect of particle size, sintering temperature and sintering time on the properties of Al–Al2O3 composites, made by powder metallurgy, Journal of Materials Processing Technology, 2009. 209: 5387–5393.
  • 6. Rahimian, M., Parvin, N., Ehsani., N., The effect of production parameters on microstructure and wear resistance of powder metallurgy Al–Al2O3 composite, Materials and Design, 2011. 32: 1031–1038.
  • 7. Arslan, G., Kalemtaş, A.,2Tunçer, E., Yeşilay, S., Emdirme Sonrası Isıl İşlemlerin B4C-Al Kompozitlerin Mikro Yapı ve Özelliklerine Etkileri, Anadolu Üniversitesi Bilim ve Teknoloji Dergisi, 2009. 10(1): 267-276.
  • 8. Cafri, M., Dilman, H., Dariel, M. P., Frage, N., Boron carbide/magnesium composites: Processing, microstructure and Properties, Journal of the European Ceramic Society, 2012. 32: 3477–3483.
  • 9. Abdizadeh, H., Ebrahimifard, R., Baghchesara, M. A., Investigation of microstructure and mechanical properties of nano MgO reinforced Al composites manufactured by stir casting and powder metallurgy methods: A comparative study, Composites: Part B, 2014. 56: 217–221.
  • 10. Karabulut, H., Çıtak, R., Çinici, H., “Mekanik Alaşımlama Süresinin Al + % 10 Al2O3 Kompozitlerde Eğme Dayanımına Etkisi”, Gazi Üniv. Müh. Mim. Fak. Der., 2013. 28(3): 635-643.
  • 11. Setoudeh, N., and Welham, N. J., Formation of zirconium diboride (ZrB2) by room temperature mechanochemical reaction between ZrO2, B2O3 and Mg, Journal of Alloys and Compounds, 2006. 420: 225–228.
  • 12. Suryanarayana, C., Mechanical alloying and milling, Progress in Materials Science, 2001, 46, 1-184.
  • 13. Deng, F., Xie, H. Y., Wang L., Synthesis of submicron B4C by mechanochemical method, Materials Letters, 2006. 60: 1771–1773.
  • 14. Sharifi, E. M., Karimzadeh, F., Enayati, M. H., Mechanochemical assisted synthesis of B4C nanoparticles, Advanced Powder Technology, 2011. 22: 354–358.
  • 15. Alizadeh, A., Taheri-Nassaj, E., Mechanical properties and wear behavior of Al–2 wt.% Cu alloy composites reinforced by B4C nanoparticles and fabricated by mechanical milling and hot extrusion, Materials Characterization, 2012. 67: 119-128.
  • 16. Anselmi-Tamburini, U., Munir, Z. A., Influence of Synthesis Temperature on the Defect Structure of Boron Carbide: Experimental and Modeling Studies, J. Am. Ceram. Soc., 2005. 88(6): 1382–1387.
  • 17. Anselmi-Tamburini, U., Ohyanagi, M., and Munir, Z. A., Modeling Studies of the Effect of Twins on the X-ray Diffraction Patterns of Boron Carbide, Chem. Mater., 2004. 16: 4347-4351.
  • 18. Li, Y., Zhao, Y. H., Liu, W., Zhang, Z. H., Vogt, R. G., Lavernia, E. J., Schoenung, J. M., Deformation twinning in boron carbide particles within nanostructured Al 5083/B4C metal matrix composites, Philosophical Magazine, 2010. 90(6): 783-792.
  • 19. Zheng, R., Hao, X., Yuan, Y., Wang, Z., Ameyama, K., Ma, C., Effect of high volume fraction of B4C particles on the microstructure and mechanical properties of aluminum alloy based composites, Journal of Alloys and Compounds, 2013. 576: 291–298.
  • 20. Jain, A., Anthonysamy, S., Ghosh, C., Ravindran, T. R., Divakar, R., Mohandas, E., “Electroextraction of boron from boron carbide scrap, Materials Characterization, 2013. 84: 134-141.
  • 21. Li, Y., Lin, Y. J., Xiong, Y. H., Schoenunga, J. M., and Lavernia, E. J., Extended twinning phenomena in Al–4% Mg alloys/B4C Nanocomposite, Scripta Materialia, 2011. 64: 133–136.

TEM characterization and synthesis of nanoparticle B4C by high-energy milling

Year 2019, Volume: 3 Issue: 3, 195 - 201, 15.12.2019

Hakan Gökmeşe Bulent Bostan Talha Alper Yilmaz Ufuk Tasci

https://doi.org/10.35860/iarej.630999
Cited By: 4

Abstract

In this study, nanoparticle B4C synthesis was carried out by
high-energy milling. For this purpose, B2O3-C-Mg triple
systems were used in the reaction stoichiometric ratios as starting materials
in the experimental studies. The reduction process of B2O3
was performed using speks type milling device. The transformation of the
ceramic phase of the nanoparticle B4C by XRD analysis was examined.
In terms of microstructural characterization of its powder shape and
morphology, TEM (imaging and selected area diffraction pattern) investigations
were conducted. The product synthesized by the leaching process was cleaned
from MgO/B4C impurities and the production of the nanoparticle B4C
was performed. After leaching processes, it was determined that some of the
synthesized powders were below 50 nm, while others varied between the ranges of
50-350 nm. In TEM examinations of B4C particles carried out after
leaching process, it was seen that there were twin formations observed as
planar error. Depending on the d values calculated by solving the TEM
diffraction patterns, the planes represented by nano-sized B4C
particles were determined.

Keywords

TEM Diffraction pattern B4C Nanoparticle Synthesis

References

  • 1. Sivasankaran, S., Sivaprasad, K., Narayanasamy, R., Satyanarayana, P.V., X-ray peak broadening analysis of AA 6061100 −x−x wt.% Al2O3 nanocomposite prepared by mechanical alloying, Materials Characterization, 2011. 62: 661-672.
  • 2. Khaghani-Dehaghani M.A., Ebrahimi-Kahrizsangi R., Setoudeh N., Nasiri-Tabrizi B., Mechanochemical synthesis of Al2O3–TiB2 nanocomposite powder from Al–TiO2–H3BO3 mixture, Int. Journal of Refractory Metals and Hard Materials, , 2011. 29: 244–249.
  • 3. Yokoyama, T., Basic Properties and Measuring Methods of Nanoparticles, Fundamentals of Nanoparticles, 2013. Chapter 1, 5-10.
  • 4. Castro, C. L. and Mitchell, B. S. Nanoparticles from Mechanical Attrition, Functionalization and Surface Treatment of Nanoparticles, 2002. Chapter 1, 1-15.
  • 5. Rahimian, M., Ehsania, N., Parvin, N., Baharvandi, H. R., The effect of particle size, sintering temperature and sintering time on the properties of Al–Al2O3 composites, made by powder metallurgy, Journal of Materials Processing Technology, 2009. 209: 5387–5393.
  • 6. Rahimian, M., Parvin, N., Ehsani., N., The effect of production parameters on microstructure and wear resistance of powder metallurgy Al–Al2O3 composite, Materials and Design, 2011. 32: 1031–1038.
  • 7. Arslan, G., Kalemtaş, A.,2Tunçer, E., Yeşilay, S., Emdirme Sonrası Isıl İşlemlerin B4C-Al Kompozitlerin Mikro Yapı ve Özelliklerine Etkileri, Anadolu Üniversitesi Bilim ve Teknoloji Dergisi, 2009. 10(1): 267-276.
  • 8. Cafri, M., Dilman, H., Dariel, M. P., Frage, N., Boron carbide/magnesium composites: Processing, microstructure and Properties, Journal of the European Ceramic Society, 2012. 32: 3477–3483.
  • 9. Abdizadeh, H., Ebrahimifard, R., Baghchesara, M. A., Investigation of microstructure and mechanical properties of nano MgO reinforced Al composites manufactured by stir casting and powder metallurgy methods: A comparative study, Composites: Part B, 2014. 56: 217–221.
  • 10. Karabulut, H., Çıtak, R., Çinici, H., “Mekanik Alaşımlama Süresinin Al + % 10 Al2O3 Kompozitlerde Eğme Dayanımına Etkisi”, Gazi Üniv. Müh. Mim. Fak. Der., 2013. 28(3): 635-643.
  • 11. Setoudeh, N., and Welham, N. J., Formation of zirconium diboride (ZrB2) by room temperature mechanochemical reaction between ZrO2, B2O3 and Mg, Journal of Alloys and Compounds, 2006. 420: 225–228.
  • 12. Suryanarayana, C., Mechanical alloying and milling, Progress in Materials Science, 2001, 46, 1-184.
  • 13. Deng, F., Xie, H. Y., Wang L., Synthesis of submicron B4C by mechanochemical method, Materials Letters, 2006. 60: 1771–1773.
  • 14. Sharifi, E. M., Karimzadeh, F., Enayati, M. H., Mechanochemical assisted synthesis of B4C nanoparticles, Advanced Powder Technology, 2011. 22: 354–358.
  • 15. Alizadeh, A., Taheri-Nassaj, E., Mechanical properties and wear behavior of Al–2 wt.% Cu alloy composites reinforced by B4C nanoparticles and fabricated by mechanical milling and hot extrusion, Materials Characterization, 2012. 67: 119-128.
  • 16. Anselmi-Tamburini, U., Munir, Z. A., Influence of Synthesis Temperature on the Defect Structure of Boron Carbide: Experimental and Modeling Studies, J. Am. Ceram. Soc., 2005. 88(6): 1382–1387.
  • 17. Anselmi-Tamburini, U., Ohyanagi, M., and Munir, Z. A., Modeling Studies of the Effect of Twins on the X-ray Diffraction Patterns of Boron Carbide, Chem. Mater., 2004. 16: 4347-4351.
  • 18. Li, Y., Zhao, Y. H., Liu, W., Zhang, Z. H., Vogt, R. G., Lavernia, E. J., Schoenung, J. M., Deformation twinning in boron carbide particles within nanostructured Al 5083/B4C metal matrix composites, Philosophical Magazine, 2010. 90(6): 783-792.
  • 19. Zheng, R., Hao, X., Yuan, Y., Wang, Z., Ameyama, K., Ma, C., Effect of high volume fraction of B4C particles on the microstructure and mechanical properties of aluminum alloy based composites, Journal of Alloys and Compounds, 2013. 576: 291–298.
  • 20. Jain, A., Anthonysamy, S., Ghosh, C., Ravindran, T. R., Divakar, R., Mohandas, E., “Electroextraction of boron from boron carbide scrap, Materials Characterization, 2013. 84: 134-141.
  • 21. Li, Y., Lin, Y. J., Xiong, Y. H., Schoenunga, J. M., and Lavernia, E. J., Extended twinning phenomena in Al–4% Mg alloys/B4C Nanocomposite, Scripta Materialia, 2011. 64: 133–136.
There are 21 citations in total.

Details

Primary Language English
Subjects Engineering
Journal Section Research Articles
Authors

Hakan Gökmeşe 0000-0002-5125-9720

Bulent Bostan This is me 0000-0002-6114-875X

Talha Alper Yilmaz This is me 0000-0002-4316-6890

Ufuk Tasci 0000-0002-8577-443X

Publication Date December 15, 2019
Submission Date October 8, 2019
Acceptance Date November 5, 2019
Published in Issue Year 2019 Volume: 3 Issue: 3

Cite

APA Gökmeşe, H., Bostan, B., Yilmaz, T. A., Tasci, U. (2019). TEM characterization and synthesis of nanoparticle B4C by high-energy milling. International Advanced Researches and Engineering Journal, 3(3), 195-201. https://doi.org/10.35860/iarej.630999
AMA Gökmeşe H, Bostan B, Yilmaz TA, Tasci U. TEM characterization and synthesis of nanoparticle B4C by high-energy milling. Int. Adv. Res. Eng. J. December 2019;3(3):195-201. doi:10.35860/iarej.630999
Chicago Gökmeşe, Hakan, Bulent Bostan, Talha Alper Yilmaz, and Ufuk Tasci. “TEM Characterization and Synthesis of Nanoparticle B4C by High-Energy Milling”. International Advanced Researches and Engineering Journal 3, no. 3 (December 2019): 195-201. https://doi.org/10.35860/iarej.630999.
EndNote Gökmeşe H, Bostan B, Yilmaz TA, Tasci U (December 1, 2019) TEM characterization and synthesis of nanoparticle B4C by high-energy milling. International Advanced Researches and Engineering Journal 3 3 195–201.
IEEE H. Gökmeşe, B. Bostan, T. A. Yilmaz, and U. Tasci, “TEM characterization and synthesis of nanoparticle B4C by high-energy milling”, Int. Adv. Res. Eng. J., vol. 3, no. 3, pp. 195–201, 2019, doi: 10.35860/iarej.630999.
ISNAD Gökmeşe, Hakan et al. “TEM Characterization and Synthesis of Nanoparticle B4C by High-Energy Milling”. International Advanced Researches and Engineering Journal 3/3 (December 2019), 195-201. https://doi.org/10.35860/iarej.630999.
JAMA Gökmeşe H, Bostan B, Yilmaz TA, Tasci U. TEM characterization and synthesis of nanoparticle B4C by high-energy milling. Int. Adv. Res. Eng. J. 2019;3:195–201.
MLA Gökmeşe, Hakan et al. “TEM Characterization and Synthesis of Nanoparticle B4C by High-Energy Milling”. International Advanced Researches and Engineering Journal, vol. 3, no. 3, 2019, pp. 195-01, doi:10.35860/iarej.630999.
Vancouver Gökmeşe H, Bostan B, Yilmaz TA, Tasci U. TEM characterization and synthesis of nanoparticle B4C by high-energy milling. Int. Adv. Res. Eng. J. 2019;3(3):195-201.

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